⚛️ Charge Redistribution in Molybdenum-Doped Cuprate Clusters

Oxidation of Cu₅MoO₁₂ exhibits behavior inconsistent with a simple localized ionic oxidation model—our sector-validated VQE simulations indicate non-local charge redistribution toward Mo d-orbitals.

Removing an electron from Cu₅MoO₁₂ causes charge density to redistribute toward Mo despite making it more positive. Our sector-validated VQE simulations indicate that Mo functions as a charge-redistribution node mediating electron flow across the cluster geometry.

🔬 Two Discoveries 📊 Sector-Validated VQE ⚡ 84× Landscape Amplification ✅ Published Data
KEY FINDINGS
Mo charge: +1.43 | Mo d-electrons: +0.27 | Correlation: −144.45 kcal/mol (cation) vs −0.18 kcal/mol (anion)

Two Discoveries, One System: Chemistry + Methodology

A
Charge Redistribution Chemistry
DOI: 10.5281/zenodo.18674751
Mo acts as charge-redistribution node: oxidation drives Cu→Mo electron donation (+0.27 d-electrons) despite Mo formal charge rising (+1.43). Correlation scales with charge polarization and open-shell character.
Published
B
VQE Sector Validation Framework
DOI: 10.5281/zenodo.18674828
Electron-sector drift detected and corrected via Hamming-weight diagnostics + number penalty. 80× purity improvement (0.240→0.003). Proposed standard for publication-quality VQE.
Published

🔬 Discovery A: Mo as Charge-Redistribution Node

System: Cu₅MoO₁₂ (anion, neutral, cation) | 20 qubits | Sector-validated VQE

Oxidation and Non-Local Charge Redistribution

Simple ionic oxidation models predict that oxidizing a transition metal complex removes electrons from the metal center, decreasing its d-orbital occupancy. For Mo-doped cuprate clusters, our sector-validated VQE simulations indicate non-local charge redistribution inconsistent with a localized ionic model.

Charge State Mo Charge Mo d-electrons Interpretation
Anion (Cu₅MoO₁₂⁻) -0.18 5.36 Reduced, closed-shell
Neutral (Cu₅MoO₁₂) -0.28 4.31 Reference state
Cation (Cu₅MoO₁₂⁺) +1.15 4.57 More positive, MORE d-electrons ⭐

Charge Redistribution Mechanism

Oxidation (neutral → cation):
Mo formal charge: +1.43 (becomes strongly positive)
Mo d-electron density: +0.27 electrons gained
Cu total charge: -0.40 (Cu donates electrons)

Mechanism: Cu → Mo charge donation compensates Mo electrostatic deficit arising from oxidation. Mo functions as a charge-redistribution node mediating electron flow across the cluster geometry, inconsistent with a simple localized ionic oxidation model.

Correlation Energy Tracks Charge Polarization and Open-Shell Character

Within this system and active space, correlation magnitude tracks charge distribution geometry and open-shell character more closely than total d-electron count.

Charge State Mo d-electrons Mo Charge Correlation Energy
Anion 5.36 -0.18 -0.18 kcal/mol
Neutral 4.31 -0.28 -14.64 kcal/mol
Cation 4.57 +1.15 -144.45 kcal/mol

The anion has the most d-electrons but the least correlation. The cation has intermediate d-electrons but correlation energy of −144.45 kcal/mol compared to −0.18 kcal/mol for the anion. The distinguishing factor is Mo charge polarization (+1.15 vs -0.18): strongly positive Mo creates highly asymmetric charge topology that drives open-shell multi-reference character.

Optimization Landscape Roughness: 84-Fold Amplification

Optimization landscape roughness (σ_tail) shows systematic correlation with HOMO-LUMO gap reduction, Mo charge polarization, and correlation energy across all three charge states.

System σ_tail (kcal/mol) HOMO-LUMO Gap (eV) Character
Anion 0.43 4.37 Ultra-smooth, closed-shell
Neutral 6.39 4.29 Smooth, moderate
Cation 36.0 3.84 Rough, open-shell singlet

Implications for Cuprate Dopant Screening

Mo's charge-redistribution behavior is not predicted by simple ionic models of oxidation state change. This framework — combining VQE energetics, Mulliken population analysis, and landscape diagnostics — provides a template for systematic dopant screening in cuprate superconductors.

Key takeaway: For transition metal dopants in ionic cluster environments, charge distribution geometry — rather than occupation numbers alone — governs the accessibility of correlated electronic states. These results are specific to the selected cluster model and active-space protocol, but provide internally consistent insight into redox-driven electronic restructuring in Mo-doped cuprate motifs.

⚙️ Discovery B: VQE Sector Validation Framework

Methodology contribution: System-agnostic detect→fix→verify workflow

A Common but Under-Quantified Failure Mode

Non-number-conserving VQE ansätze (e.g., UCCSD-type parameterizations on parity-transformed Hamiltonians) can converge to solutions exhibiting electron-sector mixing without triggering standard convergence diagnostics. Convergence criteria — energy tolerance, gradient norms — are blind to sector composition.

Case Study: Cu₅MoO₁₂ Cation (Unconstrained)

Target electron count: N = 13
Actual sector composition: P(N=13) = 86.69%
Adjacent sector contamination: P(N=12) = 7.34%, P(N=14) = 5.67%
Classification: SECTOR-MIXED ✗ (not representative of the intended electron-number sector)
Energy bias: -2.91 kcal/mol non-physical variational lowering (exceeds chemical accuracy)

Detect → Fix → Verify Workflow

1
Detect

Hamming-Weight Distribution

Compute P(N) — probability distribution over electron numbers — from final statevector. O(2ⁿ) scan, <0.1% VQE runtime overhead.

Checklist:
P(N=target) > 99%? → PURE ✓
P(N=target) < 90%? → MIXED ✗
2
Fix

Quadratic Number Penalty

Augment Hamiltonian:
H′ = H + λ(N̂ - N_target)²
Penalty strength: λ = 0.5 Ha

Result (cation):
P(N=13): 86.69% → 99.84%
Purity: 80× improvement
3
Verify

Post-Penalty Validation

Re-run sector metrics + NOON analysis. Penalty expectation ⟨λ(N̂−13)²⟩ = 0.0008 Ha (0.49 kcal/mol) — below chemical accuracy.

Verified:
Fractional NOONs: 4 → 2
(2 were sector artifacts)

Sector Validation Checklist for Publication-Quality VQE

Metric Threshold Classification
P(N=target) > 99% SECTOR-PURE ✓
P(N=target) 90–99% N-DOMINANT ⚠
P(N=target) < 90% SECTOR-MIXED ✗
Purity proxy (1 − P(N)) < 0.01 Essentially pure
⟨N⟩(1-RDM) vs ⟨N⟩(Hamming) Δ < 0.01 Consistent electron count

Proposed Standard

Hamming-weight distribution analysis is computationally inexpensive (<0.1% of VQE runtime). We recommend it as a low-overhead best practice for non-number-conserving VQE prior to publication of energetics or orbital diagnostics. The detect→fix→verify workflow is system-agnostic and applicable to any VQE implementation using parity-transformed Hamiltonians, Jordan-Wigner qubit reduction, or hardware-efficient ansätze.

⚙️ Technical Infrastructure

GPU-Accelerated VQE Implementation

These discoveries required building custom VQE infrastructure specifically designed for transition metal oxide clusters with strong correlation and open-shell character.

1. Statevector-Based Sector Monitoring

Real-time Hamming-weight monitoring during optimization. Automatic detection of sector drift before energetic comparisons are made. This is integrated into the VQE loop, not a post-processing afterthought.

2. Adaptive Number-Penalty Hamiltonian Construction

Dynamic λ selection based on sector drift magnitude. Efficient sparse Hamiltonian augmentation that preserves gradient flow. Penalty expectation tracking ensures reported energies reflect the physical Hamiltonian.

3. Multi-Seed Robustness Validation

Every charge state validated across 5 independent random seeds. Sector purity, NOON structure, and energy convergence tracked systematically. No single-run claims — all results statistically validated.

4. CASCI Benchmarking Integration

All VQE energies benchmarked against CASCI (Complete Active Space Configuration Interaction) within the same active space. Chemical accuracy validation (≤1 kcal/mol) confirmed before publication.

Applicability Beyond This System

This infrastructure enables systematic exploration and validation of quantum complexity in chemically realistic transition metal systems: CO₂ reduction catalysts, water oxidation clusters, organometallic complexes, battery cathode materials. The methodology is applicable to any strongly correlated system requiring sector-validated VQE solutions.

📊 Campaign Metrics

System
Cu₅MoO₁₂
Total Atoms
18 (1 Mo, 5 Cu, 12 O)
Qubits
20 (10 orbitals × 2)
Active Space
12-13 electrons
Total VQE Runs
26 (multi-seed)
Sector-Pure Solutions
3 (published)
Hardware
NVIDIA L40S (48GB)
Total GPU Time
~4.5 hours

📖 Access Complete Research Data

Two published datasets + validation scripts (open data)

Status: Manuscripts currently in preparation and submission.